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Beilstein J. Org. Chem. 2013, 9, 1931–1935, doi:10.3762/bjoc.9.228
Graphical Abstract
Figure 1: Structure of symbiodinolide (1).
Scheme 1: Our previous synthesis of the C79–C96 fragment 7.
Scheme 2: Retrosynthetic analysis of the C79–C97 fragment 8.
Scheme 3: Synthesis of aldehyde 20.
Scheme 4: Synthesis of PT-sulfones 23 and 24.
Scheme 5: Synthesis of the C79–C97 fragment 27.
Beilstein J. Org. Chem. 2009, 5, No. 12, doi:10.3762/bjoc.5.12
Figure 1: Structure of (R)-(−)-complanine.
Figure 2: Marine fireworm Eurythoe complanata (body length 10 cm).
Scheme 1: Total synthesis of complanine. Keys: a) 1. BH3·SMe2 (71%); 2. cat. TsOH, Et2CO (59%); 3. TsCl, pyri...